Formation of Quaternary Centers by - Macmillan Group
A 20 mL scintillation vial equipped with a magnetic stir bar was charged with the crude methyl ester intermediate from above, methanol : water ( ...
non-directed-copper-catalyzed-benzylic-ch-amination ... - ChemRxivEach vial was then opened and inserted into a 20 mL scintillation vial containing 5 mL of hexanes for vapor diffusion. The atmosphere of each two-vial ... HFIP as a versatile solvent in resorcin[n]arene synthesis... mL) was added to a 20-mL scintillation vial. UiO-66 (200 mg) and (tBuPNP)Ru(CO)HCl (1) (5.0 mg, 5.3 µmol) were added to the vial, which was then sealed. The ... Synthetic Protocols General Experimental Notes - bioRxivScintillation vials with low potassiuii. content (New England. Nuclear) are used to reduce the contribution of K-inuuceo scintillations to the background. A ...
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