WO 99/45918 - googleapis.com
Resorcinol (1 mmol) was added to a 20 mL scintillation vial equipped with a Teflon stirring bar. Next, 5 mL of hexafluoro-2-propanol were added to the flask ...
Formation of Quaternary Centers by - Macmillan GroupA 20 mL scintillation vial equipped with a magnetic stir bar was charged with the crude methyl ester intermediate from above, methanol : water ( ... non-directed-copper-catalyzed-benzylic-ch-amination ... - ChemRxivEach vial was then opened and inserted into a 20 mL scintillation vial containing 5 mL of hexanes for vapor diffusion. The atmosphere of each two-vial ... HFIP as a versatile solvent in resorcin[n]arene synthesis... mL) was added to a 20-mL scintillation vial. UiO-66 (200 mg) and (tBuPNP)Ru(CO)HCl (1) (5.0 mg, 5.3 µmol) were added to the vial, which was then sealed. The ...
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