Supporting Information - The Royal Society of Chemistry
The mixture was cooled to 0 °C using an ice/water bath and then methanesulfonyl chloride (0.53 mL, 6.84 mmol, 1.5 equiv.) was added to it dropwise. The ...
Total synthesis of the proposed structure of Sclerophytin F and ...methanesulfonyl chloride (0.25 mL, 3.2 mmol) dropwise. The mixture was stirred at ?15 °C for 30 min and the reaction was quenched by the addition of water. Supporting Information - The Royal Society of Chemistrymethanesulfonyl chloride (0.58 mL, 7.5 mmol) followed by the addition of triethyl ... J = 5.0 Hz, 1H), 3.37 (td, J = 5.5, 11.0 Hz, 1H), 2.77 (s, 3H), 2.13 ... N - HAL-RennesFrom aniline (0.465 g, 5 mmol), methanesulfonyl chloride (0.570 g, 5 mmol) and allyl bromide (0.907 g, 7.5 mmol), 3 was obtained in 88% (0.928 g ...
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